Analytical Chemistry Department Publications 2021

Rania El-Shaheny, Lateefa A. Al-Khateeb, Mahmoud El-Maghrabey. Dual-excitation in-lab-made device based on a handy UV lamp and GQDs-modified PADs for simultaneous determination of acetaminophen and its endocrine disrupting impurity 4-nitrophenol. Sensors and Actuators B: Chemical 2021, 348, 130657. https://www.sciencedirect.com/science/article/pii/S0925400521012259?via%3Dihub

Moustapha E. Moustapha, Rania M. El Gamal, and Mehnaz Kamal. Development and Validation of LC-ESI-MS/MS Method for the Determination of Alfuzosin in Human Plasma. Journal of Analytical Chemistry, 2021, 76, 1327–1335. https://link.springer.com/article/10.1134/S1061934821110095

Asmaa Kamal El-Deen and Kuniyoshi Shimizu. Deep Eutectic Solvents as Promising Green Solvents in Dispersive Liquid–Liquid Microextraction Based on Solidification of Floating Organic Droplet: Recent Applications, Challenges and Future Perspectives. Molecules 2021, 26, 7406. https://www.mdpi.com/1420-3049/26/23/7406

M. M. Tolba and M. M. Salim. Insights for applying erythrosine B as a green fluorescence probe for estimation of anticancer tamoxifen and its analog; clomiphene in nanogram concentration. Spectrochimica Acta Part A: Molecular and Biomolecular Spectroscopy. 263, 2021, 120156. https://www.sciencedirect.com/science/article/pii/S1386142521007332?via%3Dihub

Shymaa M. Abd Elhaleem, Fawzi Elsebaei, Shereen Shalan, Fathalla Belal. Utilization of Localized Surface Plasmon Resonance of Silver Nanoparticles for the Spectrofluorimetric Estimation of Oxymetazoline in Dosage Forms: Application to Aqueous Humor. Journal of Fluorescence 2021, 31, 1871–1881. https://link.springer.com/article/10.1007/s10895-021-02812-2

Heba Elmansi, Nora Elsayed, Fathalla Belal. Novel approach for chromatographic separation of atracurium and thiopental using factorial model. Microchemical Journal 170, 2021, 106751. https://www.sciencedirect.com/science/article/pii/S0026265X21008377?via%3Dihub

Mohamed Ibrahim Halawa, Qing Xia, and Bing Shi Li. An ultrasensitive chemiluminescent biosensor for tracing glutathione in human serum using BSA@AuNCs as a peroxidase-mimetic nanozyme on a luminol/artesunate system. J. Mater. Chem. B, 2021, 9, 8038-8047. DOI https://pubs.rsc.org/en/content/articlelanding/2021/TB/D1TB01343B

Mahmoud El-Maghrabey, Hajime Suzuki, Naoya Kishikawa, Naotaka Kuroda. A sensitive chemiluminescence detection approach for determination of 2,4-dinitrophenylhydrazine derivatized aldehydes using online UV irradiation – luminol CL reaction. Application to the HPLC analysis of aldehydes in oil samples. Talanta 233, 2021, 122522. https://www.sciencedirect.com/science/article/pii/S0039914021004434?via%3Dihub

M. M. Tolba, F. Belal, and M. M. Salim. Eco-friendly fluorimetric approaches for the simultaneous estimation of the co-administered ternary mixture: etoposide, moxifloxacin and nalbuphine. R. Soc. Open Sci. 2021, 8: 210683.https://royalsocietypublishing.org/doi/10.1098/rsos.210683

Rania El-Shaheny, Fathalla Belal, Yasser El-Shabrawy, Mahmoud El-Maghrabey, Nanostructures-based sensing strategies for hydrogen sulfide. Trends in Environmental Analytical Chemistry 31, 2021, e00133. https://www.sciencedirect.com/science/article/pii/S2214158821000209?via%3Dihub

Rania El-Shaheny, Lateefa A. Al-Khateeb, Mohamed A. El Hamd, Mahmoud El-Maghrabey, Correction pen as a hydrophobic/lipophobic barrier plotter integrated with paper-based chips and a mini UV-torch to implement all-in-one device for determination of carbazochrome. Analytica Chimica Acta 1172, 2021, 338684. https://www.sciencedirect.com/science/article/pii/S0003267021005109?via%3Dihub

Heba Abdel-Aziz, M. M. Tolba, N. El-Enany, F. A. Aly and M. E. Fathy Green and sensitive spectrofluorimetric method for the determination of two cephalosporins in dosage forms. R. Soc. Open Sci. 2021, 8: 210329. https://royalsocietypublishing.org/doi/10.1098/rsos.210329

Aya Roshdy, Heba Elmansi, Shereen Shalan, Amina El-Brashy. New spectroscopic methods for determination of dexlansoprazole using mercurochrome. Luminescence 2021, 36, p. 1181-1188. DOI:https://pubmed.ncbi.nlm.nih.gov/33724687/

Mohamed Hefnawy et al., Rapid and sensitive LC-MS/MS method for the enantioanalysis of verapamil in rat plasma using superficially porous silica isopropyl-cyclofructan 6 chiral stationary phase after SPE: Application to a stereoselective pharmacokinetic study. Journal of Pharmaceutical and Biomedical Analysis 201, 2021, 114108.https://www.sciencedirect.com/science/article/pii/S0731708521002193?via%3Dihub

Nora A. Abdalah, Mona E. Fathy, Manar M. Tolba,Amina M. El-Brashy and Fawzia A. Ibrahim. Green spectrofluorimetricassay of dantrolene sodiumvia reduction method:application to contentuniformity testing. R. Soc. Open Sci. 2021, 8: 210562. https://royalsocietypublishing.org/doi/10.1098/rsos.210562

Amal A. El-Masry, Dalia R. El-Wasseef, Manal Eid, Ihsan A. Shehata, and Abdallah M. Zeid. Quantitative proton nuclear magnetic resonance method for simultaneous analysis of fluticasone propionate and azelastine hydrochloride in nasal spray formulation. R. Soc. Open Sci. 2021, 8: 210483. https://royalsocietypublishing.org/doi/10.1098/rsos.210483

Galal Magdy, Ahmed F. Abdel Hakiem, Fathalla Belal, Ahmed M. Abdel-Megied. Salmon sperm DNA binding study to cabozantinib, a tyrosine kinase inhibitor: Multi-spectroscopic and molecular docking approaches. International Journal of Biological Macromolecules 182, 2021, 1852-1862. https://www.sciencedirect.com/science/article/pii/S0141813021011454?via%3Dihub

Heba Elmansi, Adel Ehab Ibrahim, Ibraam E. Mikhail, and Fathalla Belal. Green and sensitive spectrofluorimetric determination of Remdesivir, an FDA approved SARS-CoV-2 candidate antiviral; application in pharmaceutical dosage forms and spiked human plasma. Anal. Methods, 2021,13, 2596-2602. https://pubs.rsc.org/en/content/articlelanding/2021/AY/D1AY00469G

Ibraam E. Mikhail, Masoomeh Tehranirokh, Andrew A. Gooley, Rosanne M. Guijt, Michael C. Breadmore. Hyphenated sample preparation-electrospray and nano-electrospray ionization mass spectrometry for biofluid analysis. Journal of Chromatography A 1646, 2021, 462086. https://www.sciencedirect.com/science/article/pii/S0021967321002107?via%3Dihub

Galal Magdy, Ahmed F. Abdel Hakiem, Fathalla Belal, Ahmed M. Abdel-Megied. A novel quality by design approach for development and validation of a green reversed-phase HPLC method with fluorescence detection for the simultaneous determination of lesinurad, febuxostat, and diflunisal: Application to human plasma. Journal of Separation Science 2021, 44, p. 2177-2188. DOI:https://analyticalsciencejournals.onlinelibrary.wiley.com/doi/10.1002/jssc.202100016

Ibraam E. Mikhail, Heba Elmansi, Fathalla Belal, Adel Ehab Ibrahim. Green micellar solvent-free HPLC and spectrofluorimetric determination of favipiravir as one of COVID-19 antiviral regimens. Microchemical Journal 165, 2021, 106189. https://www.sciencedirect.com/science/article/pii/S0026265X21002733?via%3Dihub

Sona Barghash, Heba Elmansi, Sawsan Abd El-Razeq, Fathalla Belal. Novel spectrofluorimetric technique for determination of amoxicillin and ethopabate in chicken tissues, liver, kidney, eggs, and feed premix. Luminescence 2021, 36, p. 875-884.
https://doi-org.ezproxy.utas.edu.au/10.1002/bio.3999

Heba Abd El-Aziz, M. E .Fathy, N. El-Enany, F. A. Aly, M. M. Tolba Investigation of some univariate and multivariate spectrophotometric methods for concurrent estimation of Vancomycin and Ciprofloxacin in their laboratory prepared mixture and application to biological fluids. Spectrochimica Acta Part A: Molecular and Biomolecular Spectroscopy 253, 2021, 119570. https://www.sciencedirect.com/science/article/pii/S1386142521001463?via%3Dihub

Zeid, A.M., Abdelazim, A.H., Shahin, M. Simultaneous spectrophotometric quantitative analysis of elbasvir and grazoprevir using assisted chemometric models. Spectrochimica Acta - Part A: Molecular and Biomolecular Spectroscopy. 2021, 252, 119505. https://www.sciencedirect.com/science/article/pii/S1386142521000810?via%3Dihub

Salim, M.M., El Sharkasy, M.E., Belal, F., Walash, M. Multi-spectroscopic and molecular docking studies for binding interaction between fluvoxamine and human serum albumin. Spectrochimica Acta - Part A: Molecular and Biomolecular Spectroscopy 2021, 252, 119495. https://www.sciencedirect.com/science/article/pii/S1386142521000718?via%3Dihub

Magdy, G., Abdel Hakiem, A.F., Belal, F., Abdel-Megied, A.M. Green one-pot synthesis of nitrogen and sulfur co-doped carbon quantum dots as new fluorescent nanosensors for determination of salinomycin and maduramicin in food samples. Food Chemistry. 2021, 343, 128539. DOI:https://pubmed.ncbi.nlm.nih.gov/33183875/

Khalid A.M. Attia, Nasr M.El-Abasawi, Ahmed El-Olemy, Ahmed H. Abdelazim, Abdelrahman I.Goda, Mohammed Shahin, Abdallah M. Zeid. Simultaneous spectrophotometric quantitative analysis of velpatasvir and sofosbuvir in recently approved FDA pharmaceutical preparation using artificial neural networks and genetic algorithm artificial neural networks. Spectrochimica Acta - Part A: Molecular and Biomolecular Spectroscopy 2021, 251, 119465. DOI: https://pubmed.ncbi.nlm.nih.gov/33503564/

Mansour, N.M., El-Sherbiny, D.T., Ibrahim, F.A., El Subbagh, H.I. Development of an Inexpensive, sensitive and green HPLC method for the simultaneous determination of brivaracetam, piracetam and carbamazepine; application to pharmaceuticals and human plasma. Microchemical Journal 2021, 163, 105863. https://www.sciencedirect.com/science/article/pii/S0026265X20338054?via%3Dihub

Magdy, G., Belal, F.F., Abdel-Megied, A.M., Abdel Hakiem, A.F. Micelle-Enhanced conventional and synchronous spectrofluorimetric methods for the simultaneous determination of lesinurad and febuxostat: Application to human plasma. Spectrochimica Acta - Part A: Molecular and Biomolecular Spectroscopy 2021, 248, 119239. https://www.sciencedirect.com/science/article/pii/S138614252031218X?via%3Dihub

Sherbiny, D.E.L., Wahba, M.E.K. OFAT versus DOE as two optimization protocols for the chromatographic analysis of some OTC pharmaceuticals carrying negative cardiovascular effects and administered by pregnant and breast-feeding females: Application to dose dependent effect. Acta Chromatographica 2021, 33 (1), pp 11 – 24. https://akjournals.com/view/journals/1326/33/1/article-p11.xml

Tolba, M.M., Salim, M.M. Inclusive study for segregation of two commonly used anticancer drugs with tramadol: Applying a green fluorimetric strategy to pharmaceutical dosage forms and human plasma. Microchemical Journal 2021, 162, 105859. DOI:https://www.researchgate.net/publication/347664509_Inclusive_study_for_segregation_of_two_commonly_used_anticancer_drugs_with_tramadol_Applying_a_green_fluorimetric_strategy_to_pharmaceutical_dosage_forms_and_human_plasma

Al Shehri, Z.S., Derayea, S.M., El-Maghrabey, M.H., El Hamd, M.A. A Flavin Derivative-Based Fluorometric Analysis for the Diabetes Mellitus Inducer, Alloxan, for Its Follow-up in Flour and Flour-Derived Food. Food Analytical Methods 14 (3), pp. 2021, 473 – 484. https://link.springer.com/article/10.1007/s12161-020-01890-5

Lateefa A.Al-Khateeb, Mona A.Al-zahrani, Mohamed A.El Hamd, MahmoudEl-Maghrabey, Fatimah A.Dahas, RaniaEl-Shaheny. High-temperature liquid chromatography for evaluation of the efficiency of multiwalled carbon nanotubes as nano extraction beds for removal of acidic drugs from wastewater. Greenness profiling and comprehensive kinetics and thermodynamics studies. Journal of Chromatography A 2021, 1639, 461891. https://www.sciencedirect.com/science/article/pii/S0021967321000157?via%3Dihub

Abou-Taleb, N.H., El-Enany, N.M., El-Sherbiny, D.T., El-Subbagh, H.I. Spider diagram and Analytical GREEnness metric approach for assessing the greenness of quantitative 1H-NMR determination of lamotrigine: Taguchi method based optimization. Chemometrics and Intelligent Laboratory Systems 2021, 209, 104198. https://www.sciencedirect.com/science/article/pii/S016974392030633X?via%3Dihub

El-Maghrabey, M., Kishikawa, N., Kamimura, S., Ohyama, K., Kuroda, N. Design of a dual functionalized chemiluminescence ultrasensitive probe for quinones based on their redox cycle. Application to the determination of doxorubicin in lyophilized powder and human serum. Sensors and Actuators, B: Chemical 2021, 329, 129226. https://www.sciencedirect.com/science/article/pii/S0925400520315665?via%3Dihub

Yousef A.Bin Jardana, Khaled Mohamed, Nagwan Abbas, Manal El-Gendy, Nawaf Alsaif, Mohammed Alanazi, Mostafa Mohammed, Mohammed Abounassif, Mohamed Hefnawy. Development and validation of GC–MS method for determination of methcathinone and its main metabolite in mice plasma and brain tissue after SPE: Pharmacokinetic and distribution study. Journal of Pharmaceutical and Biomedical Analysis 2021, 194, 113798. DOI:https://pubmed.ncbi.nlm.nih.gov/33298381/

Abdallah M. Zeid, Jenny Jeehan M.Nasr, FathallaBelal, Mohamed I.Walash, Yoshinobu Baba, Noritada Kaji. Determination of three antiepileptic drugs in pharmaceutical formulations using microfluidic chips coupled with light-emitting diode induced fluorescence detection. Spectrochimica Acta - Part A: Molecular and Biomolecular Spectroscopy 2021, 246, 119021. https://www.sciencedirect.com/science/article/pii/S1386142520310003?via%3Dihub

Belal, F., Mabrouk, M., Hammad, S., Barseem, A., Ahmed, H. A Novel Eplerenone Ecofriendly Fluorescent Nanosensor Based on Nitrogen and Sulfur-Carbon Quantum Dots. Journal of Fluorescence 2021, 31(1), pp. 85 – 90. DOI: https://pubmed.ncbi.nlm.nih.gov/33074428/

Ahmed Elkashef, Nashwa Barakat, Sherry M. Khater, Amira Awadalla, Fathallah Belal, Ahmed M. El‐Assmy, Khaled Z. Sheir, Ahmed A. Shokeir. Effect of low‐energy shock wave therapy on intravesical epirubicin delivery in a rat model of bladder cancer. BJU International 2021, 127(1), pp. 80-89. DOI: https://pubmed.ncbi.nlm.nih.gov/32654305/

Halawa, M.I., Wu, G.X., Li, B.S. Development of luminol-based chemiluminescence approach for ultrasensitive sensing of Hg (II) using povidone-I2 protected gold nanoparticles as an efficient coreactant. Analytical and Bioanalytical Chemistry. 2021, 413 (2), pp. 649-659. https://link.springer.com/article/10.1007/s00216-020-03035-3

Abdallah M.Zeid, Jenny Jeehan M.Nasr, Fathalla Belal, Mohamed Walash, Noritada Kaji, Yoshinobu Baba. Microfluidic fast chiral separation of baclofen and phenylalanine enantiomers based on cyclodextrin-electrokinetic chromatography. Microchemical Journal 2021, 160, 105770. https://www.sciencedirect.com/science/article/pii/S0026265X20326448?via%3Dihub
TAREK ELAWADY, FAWZIA IBRAHIM, ALAA KHEDR and FATHALLA BELAL. Simultaneous determination of ezetimibe, atorvastatin and simvastatin using quadrupole LC-MS: Application to combined tablets and plasma after SPE. Acta Chromatographica 33 (2021) 3, 245–252. https://akjournals.com/view/journals/1326/33/3/article-p245.xml
Fawzia Ibrahim, Heba Elmansi , Rasha Aboshabana. Assessment of two analgesic drugs through fluorescence quenching of acriflavine as a new green methodology. Microchemical Journal, Volume 164, May 2021, 105882. https://www.sciencedirect.com/science/article/pii/S0026265X20338248?via%3Dihub
Rana Ghonim, Mohamed I. El-Awady, Manar M. Tolba1 and Fawzia Ibrahim. Green quantitative spectrofluorometric analysis of rupatadine and montelukast at nanogram scale using direct and synchronous techniques. R. Soc. Open Sci. 2021, 8: 211196. https://royalsocietypublishing.org/doi/10.1098/rsos.211196

Analytical Chemistry Department Publications 2021

Rana Ghonim, Mohamed I. El-Awady, Manar M. Tolba1 and Fawzia Ibrahim. Green quantitative spectrofluorometric analysis of rupatadine and montelukast at nanogram scale using direct and synchronous techniques. R. Soc. Open Sci. 2021, 8: 211196. https://royalsocietypublishing.org/doi/10.1098/rsos.211196

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